Spectrophotometric determination of uric acid in urine with 7-chloro-4-nitrobenzofrazane
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Spectrofluorimetric and spectrophotometric determination of gliclazide in pharmaceuticals by derivatization with 4-chloro-7-nitrobenzo-2-oxa-1,3-diazole.
Accurate, sensitive, and simple spectrophotometric and spectrofluorimetric methods were developed for the determination of gliclazide in pharmaceutical formulations and biological fluids. Both methods are based on a coupling reaction between gliclazide and 4-chloro-7-nitrobenzo-2-oxa-1,3-diazole in borate buffer, pH 7.8, in which a yellow reaction product that can be measured spectrophotometric...
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Since Thiamine the first discovered vitamin among B complex vitamins is considered as an essential nutrient [1], and used for treatment of many disorders and diseases [2]; and because it is included as a component of different multi-vitamins, a variety of analytical methods have been proposed for its determination in pharmaceutical formulations. Those methods include flow injection analysis (FI...
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A simple and rapid method has been developed for the determination of ascorbic acid in fruit and pharmaceutical products. The method is based on the measurement of the reaction rate between ammonium molybdate and ascorbic acid in acidic media. The reaction was monitored spectrophotometrically at 800 nm by fixed-time and variable-time methods. The calibration graph was linear in the range of...
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This paper describes the use of a FIA system for the automatic determination of uric acid in urine, using a tubular amperometric detector. In this system, glassy carbon electrodes of tubular configuration were activated by successive cyclical scans from 0.30 to 2.00 V versus Ag/AgCl reference electrode in 0.50 mol.L sulphuric acid solution. Samples were diluted in supporting electrolyte before ...
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We have developed a simple and precise paper chromatographic method for the determination of 4-hydroxy-3-methoxymandelic acid (VMA) in urine. Concentrations of VMA in patients with neuroblastoma were increased in comparison to controls. The linearity was excellent in the concentration range tested. The within-assay coefficient of variation for control and patient urine was less than 2.2%. ...
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ژورنال
عنوان ژورنال: BUNSEKI KAGAKU
سال: 1978
ISSN: 0525-1931
DOI: 10.2116/bunsekikagaku.27.8_463